Review Article
Open Access
Crystal structure analysisand synthesis of 4-((2(2 bromophenoxy)Phenyl)ethynyl)-N,N-diethylaniline
K. Hemanathan1, Kanagaraj Naveen2, P. T. Perumal2*, K. Sakthi Murugesan1*
1Department of Physics, Presidency College (Autonomous), Chennai-600 005, India
2Organic & Bio-organic Chemistry Division, CSIR-Central Leather Research Institute, Adyar, Chennai-600 020, India
K. Hemanathan et al /Int.J. Chemical Concepts. 2020,6(1),pp 08-12.
Abstract
Single crystals of4-((2(2-bromophenoxy)phenyl)ethynyl)-N,N-diethylanilinewere grown by
slow evaporation method and X-ray diffraction analysis reveals monoclinic P21/c space groupwith unit
cell dimensions of a = 9.0761 (9) Å, b= 7.5220(7) Å, c= 30.468 (3) Å and β= 97.921(3)o.Crystal data
were collected using BRUKER SMART APEX II CCDX-ray diffractometer. The structure was solved
by direct method and refined on F2 by full-matrixleast-squares procedure to the final R1 of 0.051 using
SHELXL programs.
Keywords
Bromophenoxy,N,N-diethylaniline,Crystal packingand crystal structure.
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